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Tomita, Ryohei; Tomita, Jumpei; Suzuki, Daisuke; Yasuda, Kenichiro; Miyamoto, Yutaka
Hosha Kagaku, (48), p.1 - 15, 2023/09
Secondary Ion Mass Spectrometry (SIMS) is the method to detect secondary ions produced by the sputtering of primary ions. SIMS is one of effective method to measure isotopic composition of particles containing nuclear material in environmental sample for safeguards. We are a group member of the International Atomic Energy Agency (IAEA)'s network of analytical laboratories and have developed analytical techniques using SIMS and other mass spectrometers for nuclear safeguards. We will introduce the principle of SIMS and analytical techniques developed by our group to measure isotopic composition of uranium particles which having a particle diameter of micron order in environmental sample for safeguards.
Tazaki, Makiko; Kimura, Takashi; Shimizu, Ryo; Tamai, Hiroshi; Nakatani, Takayoshi; Suda, Kazunori
JAEA-Review 2022-056, 54 Pages, 2023/01
JAEA-Review-2022-056.pdf:1.86MB
As part of the "Research on Factor Analysis and Technical Processes for Achieving Denuclearization" South Africa's nuclear development and denuclearization cases were investigated then analyzed from seven denuclearization factors namely (1) motivation for nuclear development, (2) internal and external situations at the time of denuclearization decision, (3) progress of nuclear development, (4) effects of sanctions, (5) incentives for denuclearization, (6) international framework for denuclearization, (7) denuclearization and verification methods. At the same time, characteristics of its denuclearization and lessons learned from the denuclearization were also analyzed. South Africa shifted its nuclear activities from research and development of "peaceful nuclear detonation" in the 1970s to developing "limited nuclear deterrence" and finally to manufacturing "transportable nuclear weapons" in the late 1980s. By then, it had completed producing six nuclear explosive devices using highly enriched uranium. However, in 1989, along with the abolition of the apartheid policy, South Africa decided denuclearization and dismantled its nuclear explosive devices and related facilities. Upon completion of dismantlement, it joined the Treaty on the Non- Proliferation of Nuclear Weapons and concluded a Comprehensive Safeguards Agreement (CSA) with the International Atomic Energy Agency (IAEA). The South Africa has remained one of the rare countries that has continued to the peaceful use nuclear energy, and its voluntary denuclearization is considered as a good example of denuclearization in the future.
Shirafuji, Masaya; Nozaki, Teo; Akutsu, Narumi*; Miyaji, Noriko; Nakamura, Hironobu
Dai-43-Kai Nihon Kaku Busshitsu Kanri Gakkai Nenji Taikai Kaigi Rombunshu (Internet), 4 Pages, 2022/11
In order to maintain transparency in the peaceful use of nuclear materials in Japan, it is important to appropriately respond to safeguards activities conducted by the IAEA/Japan. Failure to respond appropriately to these activities could have significant impacts, such as raising suspicion from the international community about the misuse of nuclear materials by not only the operators but also by Japan. In order to strengthen activities to appropriately respond to safeguards activities, JAEA has started (I) education on safeguards for all employees directly employed by JAEA, (II) lectures, (III) case studies, and (IV) standardization of procedures related to safeguards response since FY2020, following the methods used to foster nuclear security culture in the past. This report describes these specific activities.
Tomita, Ryohei; Tomita, Jumpei; Yomogida, Takumi; Suzuki, Daisuke; Yasuda, Kenichiro; Esaka, Fumitaka; Miyamoto, Yutaka
KEK Proceedings 2022-2, p.108 - 113, 2022/11
Automated Particle Measurement (APM) is the first measurement of environmental sample for safeguard purpose. APM tells us the number of particles in sample, their enrichment and their location. Precision and accuracy of APM is easily affected by particle condition. We have investigated how influential baking temperature in sample preparation are for uranium secondary ion quantity, uranium hydride generation and particle crystallinity. Our experimental results showed that baking temperature of 800
C reduced uranium secondary ion quantity to 33% compared with baking at 350C. Uranium hydride generation ratio of the sample baked at 850C was also 4 times higher than the sample baked at 350C. Baking at 850C raised only crystallinity of uranium particles. Baking sample at too high temperature caused less uranium secondary ion generation and much more uranium hydride generation. It made precision and accuracy of APM worse. In our experiment, baking at 350C is suitable for uranium particles in the safeguards sample.
Tomita, Jumpei; Tomita, Ryohei; Suzuki, Daisuke; Yasuda, Kenichiro; Miyamoto, Yutaka
KEK Proceedings 2022-2, p.154 - 158, 2022/11
Precise determination of minor U isotopes (
U and 
U) of particles from the safeguard environmental samples is powerful method for detecting the undeclared nuclear activities. In this study, preparation method of U particle was examined to utilize for the minor U isotope determination. The porous silica particles were used as the particle matrix and lutetium was mixed to the impregnation solution as U impregnation indicator for the particle picking. The result of the Scanning Electron Microscope indicated that the contacting the solution with Si particles overnight gently could produce the impregnated particles effectively rather than the mixing them with PFA stick.
Yomogida, Takumi; Kitatsuji, Yoshihiro; Miyamoto, Yutaka
KEK Proceedings 2022-2, p.148 - 153, 2022/11
The Research Group for Safeguards Analytical Chemistry is currently developing a method to analyze the chemical state of uranium particles in environmental samples collected at nuclear facilities using micro-Raman spectroscopy. The chemical state of uranium particles in environmental samples can be partially oxidized by long-term exposure to air. It is necessary to develop a method to analyze the chemical state of the entire particle. In this study, uranium dioxide stored under atmospheric conditions was analyzed by micro-Raman mapping. The Raman spectra showed that uranium peroxide was locally present in the UO
particle. The Raman peaks originating from the structure of UO around 570 cm
and 1150 cm could not be observed in the point analysis of the particle center. On the other hand, in mapping analysis, Raman peaks originating from the structure of UO can be observed from the same particle, demonstrating that Raman mapping analysis is an effective method for analyzing the chemical state of the entire particle.
Tamai, Hiroshi; Tazaki, Makiko; Shimizu, Ryo; Kimura, Takashi; Nakatani, Takayoshi; Suda, Kazunori
JAEA-Review 2021-073, 19 Pages, 2022/03
JAEA-Review-2021-073.pdf:1.51MB
As a part of "Research on Factor Analysis and Technical Process for Achieving Denuclearisation", investigation on Libya's cases of nuclear development and denuclearisation, and analysis of its characteristics have been conducted. Libya had been suspected that dictator Qadaffi had an interest in the acquisition of weapons of mass destruction (WMD) since early 1970s after his revolution. US and UK intelligence were focusing on Libya's situation; however, actual status was not revealed for a long time. In 1980s, Libya faced to economic exhaustion due to sanctions from the international community against Libya's supporting terrorism. Libya decided to abandon WMD development and its denuclearisation in early 2000s. Several factors to prompt Libya's decisions can be highlighted; economic sanctions; witnessing regime collapse of President Hussein due to Iraq War who aimed at WMD; revealing secret procurement of centrifuge equipment through the inspection of German-flagged ships by US. Libya's denuclearisation was rapidly implemented to prevent Libya from reverting to nuclear development through well-coordinated roles among main players, quick decisions by Libyan side, and warning effect of Iraqi case. International Atomic Energy Agency (IAEA) played a central role in the verification of all related facilities and activities in Libya. Through safeguards activities beyond those permitted by Additional Protocol (AP), IAEA evaluated the whole Libya's nuclear programme. The denuclearisation was successfully completed by removal of nuclear materials and related equipment from Libya. It was also revealed that Libya's technological capabilities had not well developed to utilize procured materials and equipment. Libya's case is regarded in the international community as a good practice of denuclearisation. On the other hand, Qadaffi administration was overthrown by the democratisation movement that occurred after denuclearisation. It might be understood as a miserable end
Tomita, Ryohei; Tomita, Jumpei; Yomogida, Takumi; Suzuki, Daisuke; Yasuda, Kenichiro; Esaka, Fumitaka; Miyamoto, Yutaka
KEK Proceedings 2021-2, p.146 - 150, 2021/12
no abstracts in English
Nakatani, Takayoshi; Shimizu, Ryo; Tazaki, Makiko; Kimura, Takashi; Tamai, Hiroshi; Suda, Kazunori
Dai-42-Kai Nihon Kaku Busshitsu Kanri Gakkai Nenji Taikai Kaigi Rombunshu (Internet), 4 Pages, 2021/11
Currently, JAEA is in the advancing of decommissioning own nuclear facilities, and some facilities have been handling nuclear materials. In decommissioning, it is necessary to consider rational methods while keeping nuclear non-proliferation and transparency, including treatment of radioactive waste generated from these facilities and methods for terminating safeguards. In this study, we considered the above issues regarding waste treatment with reference to the guidance of Safeguards by Design (SBD) published by the International Atomic Energy Agency (IAEA).
Kimura, Takashi; Fukui, Yasuhito; Tazaki, Makiko; Nakatani, Takayoshi; Shimizu, Ryo; Suda, Kazunori
Dai-42-Kai Nihon Kaku Busshitsu Kanri Gakkai Nenji Taikai Kaigi Rombunshu (Internet), 4 Pages, 2021/11
no abstracts in English
Tamai, Hiroshi; Mochiji, Toshiro; Senzaki, Masao*; Iwamoto, Tomonori*; Ishiguro, Yuzuru*; Kitade, Yuta; Sato, Heigo*; Suehiro, Rie*; Taniguchi, Tomihiro*; Fukasawa, Tetsuo*; et al.
Dai-41-Kai Nihon Kaku Busshitsu Kanri Gakkai Nenji Taikai Kaigi Rombunshu (Internet), 4 Pages, 2020/11
In light of recent delay of plutonium use in Japan and the increasing criticism of nuclear non-proliferation and nuclear security in the nuclear fuel cycle, the validity of these criticisms will be examined for the sustainable development of the nuclear fuel cycle policy. Issues on the view point of nuclear non-proliferation and nuclear security are examined.
Shiba, Tomooki; Tomikawa, Hirofumi; Yamaguchi, Tomoki
Dai-41-Kai Nihon Kaku Busshitsu Kanri Gakkai Nenji Taikai Kaigi Rombunshu (Internet), 4 Pages, 2020/11
Ozu, Akira; Maeda, Makoto; Komeda, Masao; Toh, Yosuke
Proceedings of 2019 IEEE Nuclear Science Symposium and Medical Imaging Conference (NSS/MIC 2019), Vol.1, p.101 - 104, 2020/08
Shiba, Tomooki; Tomikawa, Hirofumi
Nihon Kaku Busshitsu Kanri Gakkai Dai-40-Kai Nenji Taikai Puroshidhingusushu, 3 Pages, 2019/11
no abstracts in English
Nakanishi, Hiroaki; Nakasone, Suguru*
Kokusaiho Gaiko Zasshi, 117(3), p.642 - 643, 2018/11
Summary of questions and answers part of the 2018 Japan Society of International Law (JSIL) Annual Conference's Session 1: The 50th Anniversary of the Adoption of the Treaty on the Non-Proliferation of Nuclear Weapons (NPT) and Nuclear Disarmament
Nakanishi, Hiroaki; Kimura, Takashi; Shimizu, Ryo; Kitade, Yuta; Tazaki, Makiko; Tamai, Hiroshi; Suda, Kazunori
Nihon Kaku Busshitsu Kanri Gakkai Dai-39-Kai Nenji Taikai Rombunshu (Internet), 9 Pages, 2018/11
To extract the possible requirements for the Broader Conclusion (BC) drawn by the IAEA in the Member States, this study is to conduct the comparative analysis of the tendencies on the Member States from which the BC has been drawn and those from which the BC has not been drawn yet.
Kimura, Takashi; Tazaki, Makiko; Kitade, Yuta; Shimizu, Ryo; Tamai, Hiroshi; Nakanishi, Hiroaki; Suda, Kazunori
Nihon Kaku Busshitsu Kanri Gakkai Dai-39-Kai Nenji Taikai Rombunshu (Internet), 5 Pages, 2018/11
This is the summary of research result of State Level Concept (SLC) which has been developed and conducted by the IAEA and a major purpose of the research reported here is to promote the nuclear operator's understandings for the importance of Broder Conclusion drawn continuously by the IAEA under SLC.
Kitade, Yuta; Tamai, Hiroshi; Tazaki, Makiko; Shimizu, Ryo; Kimura, Takashi; Nakanishi, Hiroaki; Suda, Kazunori
Nihon Kaku Busshitsu Kanri Gakkai Dai-39-Kai Nenji Taikai Rombunshu (Internet), 9 Pages, 2018/11
Regional Safeguards is considered as one of the measures for strengthening IAEA safeguards and its concept is recognized at NPT Review Conference and also NSG Guidelines amended in 2011. This Study examines the elements for the proper establishment of Regional Safeguards.
Ozu, Akira; Maeda, Makoto; Komeda, Masao; Furutaka, Kazuyoshi; Toh, Yosuke
Nihon Kaku Busshitsu Kanri Gakkai Dai-38-Kai Nenji Taikai Rombunshu (Internet), 9 Pages, 2018/04
no abstracts in English
Tamai, Hiroshi; Tazaki, Makiko; Kitade, Yuta; Shimizu, Ryo; Suda, Kazunori
Nihon Kaku Busshitsu Kanri Gakkai Dai-38-Kai Nenji Taikai Rombunshu (Internet), 6 Pages, 2018/04
The United Kingdom, UK, in March 2017, notified the withdrawal from the European Union, EU. Since EURATOM is managed by the same organisation of EU, the withdrawal from EURATOM is considered to be unavoidable. UK has to define the regulation for the measures covered by EURATOM which include the implementing safeguards in the civil UK nuclear facilities and the nuclear cooperation agreements between EURATOM and third nations. UK experts recognise that such re-arrangements within 2-years are very tough hurdle, so that some alternative measures are proposed by industry side. For peaceful nuclear use in Japan, hindrances on the smooth transfers of nuclear materials and equipment between UK are concerned. This paper will discuss the UK withdrawal from EURATOM focused on the UK's correspondence and the potential influence on cooperation with Japan in view of nuclear non-proliferation.
